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Electron beam irradiated polyamide measured by indentation hardness

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dc.title Electron beam irradiated polyamide measured by indentation hardness en
dc.contributor.author Ovsík, Martin
dc.contributor.author Staněk, Michal
dc.contributor.author Janoštík, Václav
dc.contributor.author Řezníček, Martin
dc.relation.ispartof MM Science Journal
dc.identifier.issn 1803-1269 Scopus Sources, Sherpa/RoMEO, JCR
dc.date.issued 2018
utb.relation.volume 2018
utb.relation.issue March
dc.citation.spage 2149
dc.citation.epage 2152
dc.type article
dc.language.iso en
dc.publisher MM publishing Ltd.
dc.identifier.doi 10.17973/MMSJ.2018_03_201730
dc.relation.uri http://www.mmscience.eu/march-2018.html#201730
dc.subject polyamide en
dc.subject electron beam en
dc.subject cross-linking en
dc.subject nano-hardness en
dc.subject indentation en
dc.description.abstract Cross-linking is a process in which polymer chains are associated through chemical bonds. Radiation, which penetrated through specimens and reacted with the cross-linking agent, gradually formed cross-linking (3D net), first in the surface layer and then in the total volume, which resulted in considerable changes in specimen behaviour. This research paper deals with the utilization of electron beam irradiated Polyamide 11 on the nano-indentation test. Radiation doses of 66, 132 and 198 kGy were used for unfilled PA with the 5% crosslinking agent (triallyl isocyanurate). The measurement results indicated that ionizing beta radiation was a very effective tool for improvement of indentation hardness, indentation modulus, indentation creep and deformation works of studied polymers. The best results were achieved by irradiation at doses of 132 kGy (increase about 31%) by which the highest nano-mechanical properties of PA11 were achieved. © 2018, MM publishing Ltd. All rights reserved. en
utb.faculty Faculty of Technology
dc.identifier.uri http://hdl.handle.net/10563/1007794
utb.identifier.obdid 43878909
utb.identifier.scopus 2-s2.0-85043385382
utb.identifier.wok 000532565900005
utb.source j-scopus
dc.date.accessioned 2018-04-23T15:01:44Z
dc.date.available 2018-04-23T15:01:44Z
dc.description.sponsorship TBU in Zlin [IGA/FT/2017/010]; Ministry of Education, Youth and Sports of the Czech Republic within the National Sustainability Programme [LO1303 (MSMT-7778/2014)]; European Regional Development Fund under the project CEBIA-Tech [CZ.1.05/2.1.00/03.0089]
utb.contributor.internalauthor Ovsík, Martin
utb.contributor.internalauthor Staněk, Michal
utb.contributor.internalauthor Janoštík, Václav
utb.contributor.internalauthor Řezníček, Martin
utb.fulltext.affiliation MARTIN OVSIK, MICHAL STANEK, VACLAV JANOSTIK, MARTIN REZNICEK Tomas Bata University in Zlin Zlin, Czech Republic e-mail : [email protected] CONTACTS: Ing. Martin Ovsik, Ph.D. Ing. Michal Stanek, Ph.D. Ing. Vaclav Janostik Ing. Martin Reznicek, Ph.D. Tomas Bata University in Zlin, TGM 5555, 760 01 Zlin, Czech Republic Tel.: +420 576 035 100 [email protected] [email protected] [email protected] [email protected]
utb.fulltext.dates -
utb.fulltext.references [Behalek 2013] Behalek, L. and Dobransky, J. Conformal cooling of the injection moulds. Applied Mechanics and Materials. Vol. 308 (2013). pp. 127-132. ISSN 1660-9336. [Drobny 2003] Drobny, J. G. Radiation Technology for Polymers, CRC Press, New York, (2003). [Dobransky 2013] Dobransky, J. et al. Comparison of Cooling Variants by Simulation Software. Advanced Materials Research. Vol. 801 (2013). pp. 75-80. ISSN 1022-6680. [Dobransky 2015] Dobransky, J. et al. Solving Depressions Formed During Production of Plastic Molding. Metalurgija. Vol. 54. No. 3 (2015). pp. 496-498. ISSN 0543-5846. [Manas 2015] Manas, D. et al. Effect of low doses beta irradiation on micromechanical properties of surface layer of injection molded polypropylene composite. Radiation Physics and Chemistry, (2015) 114, pp. 25-30. [Oliver 2004] Oliver, W. C. and Pharr, G. M. Measurement of Hardness and Elastic Modulus by Instrumented Indentation. Journal of Materials Research 19 (1), (2004), 1564 – 1583. [Ovsik 2012] Ovsik, M. et al. Irradiated Polypropylene Studied by Microhardness and WAXS, Chemicke listy, 106 (2012), 507- 510. [Ovsik 2015] Ovsik, M. et al. Micro-indentation test and morphology of electron beam irradiated HDPE. Key Engineering Materials, 662, (2015), pp. 189-192. [Pharr 1998] Pharr, G. M. Measurement of mechanical properties by ultra-low load indentation. Materials Science and Engineering (1998).
utb.fulltext.sponsorship This paper is supported by the internal grant of TBU in Zlin No. IGA/FT/2017/010 funded from the resources of specific university research and by the Ministry of Education, Youth and Sports of the Czech Republic within the National Sustainability Programme project No. LO1303 (MSMT-7778/2014) and also by the European Regional Development Fund under the project CEBIA-Tech No. CZ.1.05/2.1.00/03.0089.
utb.wos.affiliation [Ovsik, Martin; Stanek, Michal; Janostik, Vaclav; Reznicek, Martin] Tomas Bata Univ Zlin, TGM 5555, Zlin 76001, Czech Republic
utb.scopus.affiliation Tomas Bata University in Zlin, Zlin, Czech Republic
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